diff --git a/maintenance_of_cold_traps/img/cold-trap_img_1.png b/maintenance_of_cold_traps/img/cold-trap_img_1.png new file mode 100644 index 0000000000000000000000000000000000000000..b0a6e992eec0d4d8773f43944f4831385984a7b7 Binary files /dev/null and b/maintenance_of_cold_traps/img/cold-trap_img_1.png differ diff --git a/maintenance_of_cold_traps/img/cold-trap_img_2.png b/maintenance_of_cold_traps/img/cold-trap_img_2.png new file mode 100644 index 0000000000000000000000000000000000000000..f3e595e392f0a2c3030586a734e4dc3343ce6fac Binary files /dev/null and b/maintenance_of_cold_traps/img/cold-trap_img_2.png differ diff --git a/maintenance_of_cold_traps/img/cold-trap_img_3.png b/maintenance_of_cold_traps/img/cold-trap_img_3.png new file mode 100644 index 0000000000000000000000000000000000000000..c1a980d17905e4f77bc64482c16b30aaaa0ac234 Binary files /dev/null and b/maintenance_of_cold_traps/img/cold-trap_img_3.png differ diff --git a/maintenance_of_cold_traps/maintenance_of_cold_traps.md b/maintenance_of_cold_traps/maintenance_of_cold_traps.md new file mode 100644 index 0000000000000000000000000000000000000000..4f4112a3149a10edf8d511de4d260eae5dff897c --- /dev/null +++ b/maintenance_of_cold_traps/maintenance_of_cold_traps.md @@ -0,0 +1,80 @@ +--- +layout: page +permalink: /internal/lab/maintenance_of_cold_traps/ +--- +# Maintenance of cold traps + +## Labconco Centrivap concentrator and cold trap + +The procedure describes the steps for routine maintenance of the Labconco Centrivap concentrators and cold traps. +This maintenance is important to preserve the integrity of the glass bottles inside the cold trap. + +**Instrument care officer** is responsible for cleaning the condenser once a year, changing the acid filter when necessary and filling the cold trap maintenance record sheet. +**The Users** are responsible for the routine maintenance of the instrument and filling the “cold trap maintenance record sheetâ€. + +## Description + +To ensure proper functioning of the centrivap concentrators and associated cold trap, a routine maintenance is necessary: + +**_Personal Protective Equipment_**: +* Lab coat +* Nitrile gloves + +1. This routine maintenance is performed by the users of the instrument. + +2. If a glass bottle is used inside the cold trap, add 99% ethanol to the stainless steel trap until the glass bottle is at least two-thirds immersed. + +3. At the end of each week, the cold trap should be switched off and the condensed solvent in the glass bottle should be discarded in the corresponding waste container. + +4. If there is any ice in the stainless steel trap (outside the glass bottle), let it melt, drain the ethanol and replace it with fresh ethanol. +To drain, use the faucet on the left side of the cold trap. + +<div align="center"> +<img src="img/cold-trap_img_1.png" height="250"> +</div> + +5. Fill the “cold trap maintenance record sheet “ (Appendix 01) + +6. Restart the cold trap at the beginning of the following week + +**Once a year, the refrigeration system condenser of the Cold trap should be cleaned.** + +**_Personal Protective Equipment_**: +* Lab coat +* Nitrile gloves +* Safety goggles + +1. This step is performed by a maintenance officer + +2. Switch off the instrument + +3. Use a vacuum cleaner with brush attachment + +4. Clean the condenser (on the left side of the cold trap) to ensure proper airflow for peak performance + +<div align="center"> +<img src="img/cold-trap_img_2.png" height="250"> +</div> + +5. Fill the “cold trap maintenance record sheet “ (Appendix 01) +When necessary, the acid cartridge (LIMS ID: 10608) should be exchanged + +* When the cartridge looks wet (see arrow on the following picture), it should be exchanged for a new one. + +<div align="center"> +<img src="img/cold-trap_img_3.png" height="250"> +</div> + +* This is done by a maintenance officer + +* Switch off the instrument + +* Unscrew the black cap out of the transparent container + +* Remove the cartridge and replace it with the new one + +* Close back the container + +* Place the old cartridge in the chemical hood for evaporation in a retention container + +* 24 hours later, trash it in a blue bin UN3291 \ No newline at end of file